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Chromaster 5610 MS detector is a new mass detector, designed for LC users, and it is different from conventional mass spectrometers. By using this detector with syringe pump, a sample solution is introduced directly to 5610 MS Detector and the mass information can be obtained easily. The system allows the confirmation of the mass information of synthetic compounds or simple monitoring for the compound identification when the synthetic conditions are being studied. This time, the system was used for the confirmation of the mass information on the synthetic intermediates in the following synthesis scheme, and the analysis example is introduced here.