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Chromaster 5610 MS Detector is a mass detector with new concept, designed for LC users, and it is different from conventional mass spectrometers. Organic acids greatly affect the tastes and flavors of foods and therefore, are frequently analyzed for the purpose of research and development, quality control, etc. In addition to food products, various products such as drugs, culture liquids, plating solutions, and cosmetics are being analyzed. This time, six organic acids are separated by using a HILIC column and detected by Chromaster 5610 MS detector, and the example is introduced here.